2924-15-4

2-氟苯肼鹽酸鹽(2924-15-4)核磁圖(¹HNMR)

產(chǎn)品名稱:2-氟苯肼鹽酸鹽

CAS:2924-15-4

分子式:C6H8ClFN2

分子量: 162.59

InChI:InChI=1S/C6H7FN2.ClH/c7-5-3-1-2-4-6(5)9-8;/h1-4,9H,8H2;1H

InChIKey: VFZYLSYYMHFPSY-UHFFFAOYSA-N

Smiles:C1(NN)=CC=CC=C1F.Cl

Mass

MS-NW-7334          
o-fluorophenylhydrazine hydrochloride
C6H7FN2 HCl         (Mass of molecular ion:    126)

   Source Temperature: 150 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      18.0       3.9
      28.0       1.3
      29.0       2.2
      31.0       1.9
      35.0       2.9
      36.0      24.0
      37.0       1.2
      38.0       8.0
      39.0       3.0
      50.0       4.6
      51.0       8.3
      52.0       2.8
      53.0       2.3
      56.0       1.4
      57.0       8.2
      61.0       1.2
      62.0       2.1
      63.0       7.0
      64.0       1.4
      68.0       1.4
      69.0       1.8
      70.0       2.7
      74.0       2.2
      75.0       5.7
      76.0       1.6
      77.0       8.1
      78.0       5.7
      79.0       1.4
      81.0       3.3
      82.0       6.4
      83.0      52.0
      84.0       4.2
      89.0       1.8
      90.0       1.2
      94.0       1.0
      95.0       5.6
      96.0       8.9
      97.0       4.1
      98.0       1.6
     105.0       1.4
     108.0       1.8
     109.0      10.7
     110.0      43.1
     111.0       9.5
     125.0       4.5
     126.0     100.0
     127.0       7.7
     299.0       1.2

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₆ H₇ F N₂	0.041 g : 0.5 ml DMSO-d₆
o-fluorophenylhydrazine hydrochloride

    Assign.     Shift(ppm)

      A            10.5
      B             8.33
      C             7.279
      D             7.197
      E             7.144
      G             6.979

     Hz     ppm     Int.

   4199.82  10.509    850
   3330.70   8.335    223
   2918.94   7.304    400
   2917.48   7.301    434
   2909.42   7.280    841
   2905.20   7.270     95
   2902.09   7.262    590
   2900.62   7.258    572
   2887.44   7.225    509
   2886.15   7.222    557
   2879.38   7.205    626
   2878.10   7.202    675
   2875.53   7.196    542
   2874.25   7.192    596
   2867.47   7.175    616
   2866.19   7.172    712
   2863.08   7.164    554
   2862.16   7.162    546
   2855.57   7.146   1000
   2854.83   7.144    931
   2847.69   7.126    531
   2846.59   7.123    502
   2799.15   7.005    345
   2797.69   7.001    362
   2794.20   6.992    381
   2792.74   6.988    450
   2791.64   6.986    492
   2791.09   6.984    489
   2789.99   6.982    496
   2786.70   6.973    501
   2785.23   6.970    513
   2783.76   6.966    343
   2782.12   6.962    277
   2778.64   6.953    261
   2777.17   6.950    240

KBr disc