2958-36-3

2-氨基-2',5-二氯二苯酮(2958-36-3)紅外圖譜(IR1)

產(chǎn)品名稱:2-氨基-2',5-二氯二苯酮

CAS:2958-36-3

分子式:C13H9Cl2NO

分子量: 266.12

InChI:InChI=1S/C13H9Cl2NO/c14-8-5-6-12(16)10(7-8)13(17)9-3-1-2-4-11(9)15/h1-7H,16H2

InChIKey: KWZYIAJRFJVQDO-UHFFFAOYSA-N

Smiles:C(C1=CC(Cl)=CC=C1N)(C1=CC=CC=C1Cl)=O

Mass

MS-NW-9701          
2-amino-2',5-dichlorobenzophenone
C13H9Cl2NO          (Mass of molecular ion:    265)

   Source Temperature: 150 °C
   Sample Temperature:  80 °C
   Direct, 75 eV

      39.0       1.0
      50.0       1.2
      51.0       1.3
      52.0       1.4
      62.0       1.3
      63.0       4.8
      64.0       1.5
      65.0       1.1
      73.0       1.7
      74.0       1.4
      75.0       7.2
      76.0       1.3
      82.5       1.4
      83.5       1.0
      90.0       6.4
      91.0       2.8
      99.0       7.4
     100.0       1.1
     100.5       1.9
     101.0       2.8
     111.0      14.6
     112.0       1.2
     113.0       5.2
     115.0       5.5
     115.5       1.0
     116.0       1.8
     125.0       1.6
     126.0      14.0
     127.0       1.7
     128.0       4.6
     138.0       1.1
     139.0      22.2
     140.0       3.4
     141.0       6.6
     153.0       2.4
     154.0      28.9
     155.0       3.1
     156.0       9.6
     164.0       1.6
     165.0       1.1
     166.0       6.2
     167.0       8.9
     168.0       1.5
     194.0       1.8
     195.0      24.9
     196.0       3.8
     200.0       1.7
     201.0       5.2
     202.0       2.5
     203.0       1.9
     229.0      12.1
     230.0     100.0
     231.0      18.2
     232.0      32.7
     233.0       4.7
     236.0       4.1
     238.0       2.6
     248.0       3.7
     250.0       2.4
     264.0      18.6
     265.0      56.4
     266.0      19.9
     267.0      36.6
     268.0       7.0
     269.0       6.2

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₃ H₉ Cl₂ N O	0.036 g : 0.5 ml CDCl₃
2-amino-2',5-dichlorobenzophenone

    Assign.     Shift(ppm)

      A             7.459
      B             7.414
      C             7.341
      D             7.300
      E             7.225
      F             7.114
      G             6.669
      J             6.42

     Hz     ppm     Int.

   2987.43   7.476    274
   2986.94   7.474    299
   2985.84   7.472    372
   2983.40   7.466     74
   2979.61   7.456    619
   2979.00   7.455    685
   2978.03   7.452    748
   2977.54   7.451    705
   2971.31   7.435    401
   2969.60   7.431    417
   2964.11   7.417    617
   2962.40   7.413    629
   2958.74   7.404     81
   2956.30   7.398    368
   2954.35   7.393    381
   2950.20   7.382    410
   2948.61   7.378    397
   2946.78   7.374     83
   2942.75   7.364    663
   2941.28   7.360    683
   2937.87   7.352     76
   2937.38   7.350     75
   2935.55   7.346    374
   2934.08   7.342    354
   2930.42   7.333     39
   2925.17   7.320     52
   2921.14   7.310    601
   2920.65   7.309    644
   2919.31   7.305    584
   2918.82   7.304    578
   2913.33   7.290    425
   2911.87   7.287    359
   2897.46   7.250     38
   2893.31   7.240    547
   2890.87   7.234    609
   2884.52   7.218    590
   2881.96   7.212    656
   2844.36   7.118    985
   2841.92   7.112    911
   2675.29   6.695     30
   2669.68   6.681   1000
   2666.99   6.674     84
   2665.41   6.670     63
   2663.70   6.666     74
   2660.77   6.658    953
   2586.55   6.473    311

in CDCl3