376609-78-8

4-正十八烷氧基聯(lián)苯(376609-78-8)質(zhì)譜(MS)

產(chǎn)品名稱:4-正十八烷氧基聯(lián)苯

CAS:376609-78-8

分子式:C30H46O

分子量: 422.69

Mass

MS-KW-0574          
4-octadecyloxybiphenyl
C30H46O             (Mass of molecular ion:    422)

   Source Temperature: 170 °C
   Sample Temperature: 140 °C
   Direct, 75 eV

      29.0       2.7
      41.0       7.0
      42.0       1.0
      43.0      12.0
      55.0      10.8
      56.0       1.6
      57.0       8.8
      69.0       7.2
      70.0       1.2
      71.0       3.6
      83.0       4.8
      85.0       1.9
      97.0       3.2
     111.0       1.2
     115.0       1.5
     141.0       3.1
     152.0       1.8
     153.0       2.9
     169.0       2.6
     170.0     100.0
     171.0      14.6
     172.0       1.2
     183.0       1.9
     422.0      23.2
     423.0       7.7
     424.0       1.3

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₃₀H₄₆O	0.039 g : 0.5 ml CDCl₃
4-(octadecyloxy)biphenyl

    Assign.     Shift(ppm)

     A           7.540
     B           7.504
     C           7.396
     D           7.285
     E           6.955
     F           3.978
     G           1.793
     J           1.462
     K           1.26
     L           0.878

     Hz     ppm     Int.

   3019.54   7.553     64
   3018.19   7.550     78
   3016.12   7.545     28
   3012.09   7.535     50
   3011.11   7.532     93
   3009.89   7.529     86
   3007.21   7.523     23
   3004.16   7.515    123
   3001.96   7.509     43
   2997.44   7.498     43
   2995.37   7.493    134
   2992.31   7.485     19
   2964.36   7.415     54
   2962.53   7.411     24
   2956.91   7.397     93
   2950.69   7.381     28
   2948.98   7.377     56
   2919.44   7.303     24
   2918.10   7.300     41
   2916.88   7.297     26
   2912.60   7.286     21
   2910.77   7.281     49
   2908.94   7.277     19
   2904.67   7.266     16
   2903.45   7.263     24
   2902.10   7.260     14
   2787.48   6.973     19
   2784.43   6.965    125
   2782.35   6.960     41
   2777.84   6.949     39
   2775.64   6.943    118
   2772.59   6.936     17
   1596.93   3.995     61
   1590.34   3.978    125
   1583.75   3.962     62
    724.00   1.811     36
    717.05   1.794     42
    708.99   1.774     40
    702.52   1.758     18
    592.17   1.482     22
    584.97   1.464     31
    577.03   1.444     26
    539.56   1.350     29
    503.06   1.259   1000
    357.92   0.896     60
    351.32   0.879    182
    344.24   0.862     72

in CDCl3