38051-57-9

癸基二甲基氯硅烷(38051-57-9)質(zhì)譜(MS)

產(chǎn)品名稱:癸基二甲基氯硅烷

CAS:38051-57-9

分子式:C12H27ClSi

分子量: 234.88

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-9197          
chlorodecyldimethylsilane
C12H27ClSi          (Mass of molecular ion:    234)

   Source Temperature: 220 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      27.0       2.4
      29.0       4.9
      39.0       2.0
      41.0       7.6
      42.0       2.2
      43.0      11.5
      55.0       3.8
      56.0       2.4
      57.0       6.7
      58.0       1.0
      59.0       2.8
      63.0       2.2
      65.0       3.6
      67.0       2.0
      69.0       2.4
      70.0       2.2
      71.0       5.5
      78.0       1.1
      79.0       6.2
      81.0       2.5
      83.0       3.4
      84.0       1.5
      85.0       6.0
      92.0       1.6
      93.0     100.0
      94.0       7.8
      95.0      35.3
      96.0       2.7
      97.0       3.8
      98.0       1.0
      99.0       1.0
     105.0       1.2
     107.0       3.6
     109.0       1.3
     111.0       2.2
     119.0       3.0
     121.0      17.4
     122.0       1.7
     123.0       5.7
     133.0       2.5
     135.0       2.8
     137.0       1.1
     139.0       1.1
     140.0       4.5
     147.0       4.0
     149.0       2.6
     219.0      18.2
     220.0       3.0
     221.0       6.4

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₂ H₂₇ Cl Si	0.05 ml : 0.5 ml CDCl₃
chlorodecyldimethylsilane

    Assign.     Shift(ppm)

      A             1.41
      B             1.27
      C             0.882
      D             0.812
      E             0.395

     Hz     ppm     Int.

    562.38   1.408     35
    505.98   1.267    452
    359.25   0.899     83
    355.83   0.891     39
    352.54   0.883    265
    345.46   0.865    100
    332.76   0.833     70
    325.07   0.814     50
    316.53   0.793     80
    161.50   0.405     81
    158.08   0.396   1000
    154.66   0.387     87

in CDCl3