3855-32-1

N-[3-(二甲氨基)丙基]-N,N’,N’-三甲基-1,3丙二胺(3855-32-1)核磁圖(¹³CNMR)

產(chǎn)品名稱:N-[3-(二甲氨基)丙基]-N,N’,N’-三甲基-1,3丙二胺

CAS:3855-32-1

分子式:C11H27N3

分子量: 201.35

InChI:InChI=1S/C11H27N3/c1-12(2)8-6-10-14(5)11-7-9-13(3)4/h6-11H2,1-5H3

InChIKey: SKCNNQDRNPQEFU-UHFFFAOYSA-N

Smiles:C(N(CCCN(C)C)C)CCN(C)C

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-9002          
N-(3-(dimethylamino)propyl)-N,N',N'-trimethyltrimethylenediamine
C11H27N3            (Mass of molecular ion:    201)

   Source Temperature: 200 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       1.5
      27.0       1.0
      28.0       2.6
      29.0       1.3
      30.0       3.8
      41.0       3.2
      42.0      13.9
      43.0       5.7
      44.0       9.7
      45.0       1.8
      56.0       3.5
      57.0       4.9
      58.0     100.0
      59.0       4.5
      70.0      18.1
      71.0       7.2
      72.0      10.7
      82.0       2.3
      83.0       1.1
      84.0      15.8
      85.0      63.9
      86.0       8.0
      96.0       3.2
      98.0       6.1
     111.0       1.5
     113.0       1.2
     117.0       7.9
     127.0       5.0
     156.0       1.0
     201.0       7.6
     202.0       1.1

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₁ H₂₇ N₃	0.05 ml : 0.5 ml CDCl₃
N-(3-(dimethylamino)propyl)-N,N',N'-trimethyltrimethylenediamine

    Assign.     Shift(ppm)

      A             2.357
      B             2.274
      C             2.219
      D             1.640

     Hz     ppm     Int.

    952.27   2.383     33
    949.58   2.377    126
    942.02   2.358    136
    939.82   2.352     65
    934.45   2.339    134
    916.14   2.293    134
    908.81   2.275    156
    901.12   2.255    148
    887.08   2.220   1000
    670.17   1.677     40
    664.18   1.662     48
    662.60   1.658     82
    657.47   1.646     52
    655.15   1.640    131
    653.20   1.635     48
    649.17   1.625     46
    647.46   1.621     67
    646.36   1.618     47
    640.14   1.602     33

in CDCl3