4832-52-4

三(苯硫基)甲烷(4832-52-4)質(zhì)譜(MS)

產(chǎn)品名稱:三(苯硫基)甲烷

CAS:4832-52-4

分子式:C19H16S3

分子量: 340.53

Mass

MS-NW-8019          
tris(phenylthio)methane
C19H16S3            (Mass of molecular ion:    340)

   Source Temperature: 170 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      39.0       2.9
      45.0       5.5
      50.0       1.1
      51.0       7.7
      65.0       5.0
      66.0       2.3
      69.0       1.9
      77.0      13.3
      78.0       3.6
      91.0       1.5
     109.0      14.0
     110.0       5.5
     111.0       1.0
     121.0      27.3
     122.0       6.5
     123.0       1.9
     153.0      14.2
     154.0       1.5
     155.0       1.4
     165.0       1.8
     166.0       1.5
     167.0       2.7
     197.0       3.9
     198.0       1.0
     231.0     100.0
     232.0      16.0
     233.0       9.8
     234.0       1.4

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₉ H₁₆ S₃	0.053 g : 0.5 ml CDCl₃
tris(phenylthio)methane

    Assign.     Shift(ppm)

      A             7.478
      B             7.30
      C             7.29
      D             5.416
     
     ASSIGNED BY C-H COSY.

     Hz     ppm     Int.

   2995.85   7.497     88
   2993.65   7.491    451
   2992.92   7.489    279
   2991.58   7.486    238
   2990.72   7.484    302
   2989.14   7.480    386
   2987.55   7.476    164
   2985.96   7.472    531
   2984.01   7.467    527
   2980.47   7.458     74
   2979.25   7.455     49
   2977.91   7.452     30
   2930.42   7.333     58
   2929.69   7.331     47
   2928.71   7.329     43
   2925.29   7.320    209
   2923.71   7.316    126
   2922.73   7.314    149
   2921.39   7.310    467
   2920.90   7.309    522
   2920.17   7.307    367
   2919.07   7.305    572
   2915.89   7.297    790
   2914.06   7.292   1000
   2911.62   7.286    170
   2910.40   7.283    128
   2909.91   7.282    125
   2905.64   7.271     41
   2903.81   7.266     32
   2164.43   5.416    603

in CDCl3