4937-62-6

2-氨基-4-甲基二苯甲酮(4937-62-6)紅外圖譜(IR1)

產(chǎn)品名稱(chēng):2-氨基-4-甲基二苯甲酮

CAS:4937-62-6

分子式:C14H13NO

分子量: 211.26

Mass

MS-NW-7926          
2-amino-4-methylbenzophenone
C14H13NO            (Mass of molecular ion:    211)

   Source Temperature: 160 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      18.0       1.1
      27.0       1.4
      28.0       1.8
      39.0       2.8
      50.0       1.7
      51.0       6.7
      52.0       2.2
      53.0       1.8
      63.0       1.6
      65.0       1.4
      66.0       1.1
      76.0       1.5
      77.0      25.8
      78.0       3.8
      79.0       8.7
      80.0       1.0
      83.5       1.2
      89.0       1.2
      90.0       1.1
      90.5       2.8
      91.0       1.3
      91.5       1.2
     104.0       2.6
     104.5       5.5
     105.0       9.2
     105.5       1.6
     106.0      13.8
     107.0       1.3
     115.0       1.0
     134.0      41.8
     135.0       4.0
     165.0       1.2
     166.0       1.1
     167.0       3.1
     168.0       1.0
     180.0       2.5
     181.0       1.3
     182.0       4.0
     183.0       1.0
     194.0       6.0
     195.0       3.5
     196.0       1.4
     209.0       1.7
     210.0     100.0
     211.0      77.1
     212.0      11.2
     213.0       1.0

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₄ H₁₃ N O	0.050 g : 0.5 ml CDCl₃
2-amino-4-methylbenzophenone

    Assign.     Shift(ppm)

      A             7.604
      B             7.487
      C             7.433
      D             7.329
      E             6.522
      F             6.401
      G             6.13
      J             2.267

     Hz     ppm     Int.

   3046.51   7.623     33
   3044.43   7.618    204
   3043.09   7.615    257
   3041.50   7.611    130
   3038.45   7.603     87
   3036.25   7.598    354
   3034.79   7.594    273
   3002.08   7.512     54
   3000.61   7.509     32
   2997.44   7.501     38
   2994.75   7.494    170
   2992.31   7.488     53
   2988.89   7.479    101
   2987.43   7.476    161
   2985.96   7.472     76
   2978.03   7.452     61
   2976.81   7.449    202
   2976.07   7.447    261
   2974.73   7.444    107
   2970.21   7.433    195
   2968.63   7.429    300
   2966.92   7.424     75
   2963.26   7.415     54
   2961.67   7.411    132
   2960.33   7.408     72
   2933.47   7.341    222
   2925.29   7.320    232
   2606.69   6.523    215
   2562.87   6.413    121
   2562.50   6.412    120
   2561.28   6.409    116
   2554.69   6.393    115
   2554.32   6.392    116
   2553.10   6.389    112
   2451.29   6.134     95
    906.01   2.268   1000

in CDCl3