3-甲氧基芐胺(5071-96-5)核磁圖(1HNMR)
InChI:InChI=1S/C8H11NO/c1-10-8-4-2-3-7(5-8)6-9/h2-5H,6,9H2,1H3
InChIKey: GRRIMVWABNHKBX-UHFFFAOYSA-N
Smiles:C1(CN)=CC=CC(OC)=C1
-
Mass
MS-NW-5464
m-methoxybenzylamine
C8H11NO (Mass of molecular ion: 137)
Source Temperature: 260 °C
Sample Temperature: 190 °C
Reservoir, 75 eV
15.0 2.4
18.0 2.1
27.0 2.2
28.0 18.7
29.0 3.0
30.0 41.9
31.0 1.1
37.0 1.2
38.0 3.6
39.0 9.7
40.0 1.7
41.0 3.0
42.0 2.2
44.0 3.8
50.0 5.2
51.0 8.7
52.0 3.8
53.0 2.1
54.0 1.8
62.0 2.2
63.0 7.4
64.0 5.5
65.0 12.0
66.0 7.8
67.0 5.1
74.0 1.6
75.0 1.4
76.0 2.4
77.0 22.2
78.0 12.9
79.0 10.3
80.0 1.3
89.0 2.5
90.0 2.6
91.0 12.0
92.0 5.4
93.0 9.7
94.0 19.8
95.0 4.0
103.0 1.2
104.0 6.8
105.0 7.9
106.0 45.3
107.0 7.1
108.0 12.3
109.0 24.3
110.0 2.2
119.0 5.3
120.0 12.6
121.0 21.3
122.0 17.0
123.0 1.5
133.0 1.5
134.0 2.4
135.0 1.3
136.0 100.0
137.0 73.0
138.0 7.2
150.0 2.4
151.0 1.2
255.0 1.5
90 MHz in CDCl3
400 MHz in CDCl3
-
| 1H NMR |
89.56 MHz |
| C8 H11 N O
|
0.04 ml : 0.5 ml CDCl3
|
| m-methoxybenzylamine
|
 |
Assign. Shift(ppm)
A 7.22
B 6.85
C 6.84
D 6.77
E 3.82
F 3.790
G 1.49
400MHZ. : HSP-41-700
|
Hz ppm Int.
656.44 7.330 30
648.63 7.243 87
640.50 7.152 76
619.69 6.920 48
619.13 6.914 57
618.63 6.908 49
618.06 6.902 63
617.44 6.895 44
615.00 6.867 61
614.38 6.860 74
613.50 6.851 60
612.31 6.837 101
611.69 6.830 114
342.31 3.823 234
339.50 3.791 1000
133.50 1.491 415
-
| 1H NMR |
399.65 MHz |
| C8 H11 N O
|
0.05 ml : 0.5 ml CDCl3
|
| m-methoxybenzylamine
|
|
Assign. Shift(ppm)
A 7.210
B 6.85
C 6.84
D 6.755
E 3.785
F 3.752
G 1.51
90MHZ. : HSP-03-438
|
Hz ppm Int.
2890.01 7.232 81
2881.71 7.211 169
2874.15 7.192 119
2742.43 6.863 129
2742.07 6.862 131
2734.99 6.844 256
2733.64 6.841 237
2704.59 6.768 100
2702.39 6.762 91
2697.02 6.749 80
2695.56 6.745 85
2693.60 6.740 76
1512.82 3.786 376
1499.63 3.753 1000
604.13 1.512 199