5267-39-0

4-氯二苯甲胺鹽酸鹽(5267-39-0)紅外圖譜(IR2)

產品名稱:4-氯二苯甲胺鹽酸鹽

CAS:5267-39-0

分子式:C13H12ClN

分子量: 217.69

Mass

MS-IW-0011          
4-chlorobenzhydrylamine hydrochloride
C13H12ClN HCl       (Mass of molecular ion:    217)

   Source Temperature: 170 °C
   Sample Temperature: 120 °C
   Direct, 75 eV

      17.0       1.0
      18.0       5.5
      28.0      16.0
      35.0       1.8
      36.0      21.8
      38.0       7.2
      39.0       1.5
      50.0       2.3
      51.0       5.7
      52.0       1.6
      63.0       1.7
      74.0       1.0
      75.0       3.5
      76.0       3.2
      77.0      20.4
      78.0       3.4
      79.0      10.3
      81.5       1.1
      82.0       2.2
      82.5       2.0
      89.0       1.5
      89.5       1.7
      90.0       3.3
      90.5       2.8
      91.0       1.0
     102.0       1.9
     104.0      22.4
     105.0     100.0
     106.0      50.8
     107.0       3.8
     111.0       3.3
     113.0       6.0
     115.0       2.2
     138.0      14.5
     139.0      26.5
     140.0      59.0
     141.0      12.6
     142.0      17.4
     143.0       1.4
     151.0       1.0
     152.0       1.9
     153.0       1.2
     163.0       1.9
     164.0       2.2
     165.0      10.9
     166.0       5.4
     167.0       1.3
     180.0       2.9
     181.0       1.0
     182.0       5.5
     199.0       1.5
     201.0       3.1
     214.0       1.0
     216.0      13.6
     217.0      29.0
     218.0       8.3
     219.0       9.7
     220.0       1.3

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₁₃ H₁₂ Cl N	0.034 g : 0.5 ml DMSO-d₆
4-chlorobenzhydrylamine hydrochloride

    Assign.     Shift(ppm)

      A             9.46
      B             7.646
      C             7.61
      D             7.488
      E             7.412
      F             7.352
      G             5.683

     Hz     ppm     Int.

   3779.82   9.458    489
   3060.90   7.659    672
   3058.88   7.654    244
   3054.12   7.642    298
   3052.29   7.638    884
   3049.54   7.631    172
   3047.16   7.625    409
   3045.88   7.622    538
   3038.55   7.604    623
   2999.17   7.505    133
   2996.60   7.499   1000
   2994.59   7.494    291
   2989.83   7.482    279
   2988.00   7.477    786
   2985.43   7.471    101
   2971.33   7.435    195
   2970.23   7.433    294
   2968.58   7.428    120
   2963.27   7.415    673
   2961.80   7.411    341
   2955.57   7.396    448
   2944.58   7.368    176
   2943.30   7.365    297
   2942.20   7.362    183
   2938.36   7.353    113
   2936.16   7.347    362
   2933.59   7.341     82
   2929.93   7.332     75
   2928.83   7.329    109
   2927.73   7.326     62
   2272.00   5.685    565

in DMSO-d6