56746-19-1

溴代二乙基苯胺(56746-19-1)核磁圖(¹³CNMR)

產(chǎn)品名稱:溴代二乙基苯胺

CAS:56746-19-1

分子式:C10H14BrN

分子量: 228.13

InChI:InChI=1S/C10H14BrN/c1-3-7-5-9(11)6-8(4-2)10(7)12/h5-6H,3-4,12H2,1-2H3

InChIKey: BEJYDMQQZUACPW-UHFFFAOYSA-N

Smiles:C1(N)=C(CC)C=C(Br)C=C1CC

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-9359          
4-bromo-2,6-diethylaniline
C10H14BrN           (Mass of molecular ion:    227)

   Source Temperature: 260 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      27.0       2.3
      28.0       4.6
      29.0       1.0
      30.0       1.5
      39.0       4.6
      41.0       2.3
      42.0       1.7
      50.0       1.6
      51.0       5.7
      52.0       3.5
      53.0       2.9
      54.0       1.8
      58.5       6.1
      59.0       1.7
      59.5       2.7
      62.0       1.2
      63.0       3.6
      64.0       1.7
      64.5       3.0
      65.0       7.5
      65.5       6.3
      66.0       2.9
      66.5       4.4
      67.0       1.1
      71.5       1.0
      72.5       1.2
      74.0       1.3
      75.0       1.7
      76.0       1.8
      77.0       7.7
      78.0       3.6
      79.0       2.2
      89.0       3.2
      90.0       2.7
      91.0      10.2
      92.0       2.1
      93.0       1.5
      98.5       3.3
      99.5       3.2
     102.0       2.6
     103.0       4.1
     104.0       3.8
     105.0       3.3
     106.0       3.2
     115.0       9.0
     116.0       7.9
     117.0      11.9
     118.0       9.5
     119.0       7.3
     120.0       4.9
     127.0       1.1
     128.0       2.7
     129.0       2.8
     130.0      10.2
     131.0       7.0
     132.0      25.6
     133.0      71.8
     134.0       7.9
     146.0       1.4
     147.0       5.7
     148.0      10.8
     149.0       1.5
     162.0       1.1
     184.0       1.2
     197.0       2.1
     198.0       3.3
     199.0       2.0
     200.0       2.6
     210.0       1.4
     212.0     100.0
     213.0      11.2
     214.0      96.6
     215.0      10.3
     226.0       2.4
     227.0      85.4
     228.0      12.0
     229.0      83.6
     230.0       9.6

90 MHz in CDCl3

in CDCl3

¹H NMR	89.56 MHz
C₁₀ H₁₄ Br N	0.05 ml : 0.5 ml CDCl₃
4-bromo-2,6-diethylaniline

    Assign.     Shift(ppm)

      A             7.048
      B             3.58
      C             2.448
      D             1.219

     Hz     ppm     Int.

    631.06   7.047    465
    320.63   3.581     79
    231.25   2.583     88
    230.81   2.578     88
    228.25   2.549     29
    223.38   2.495    299
    215.88   2.411    341
    211.75   2.365     36
    208.75   2.331    133
    116.00   1.296    488
    108.75   1.215   1000
    104.19   1.164     58
    101.06   1.129    360