尿苷(58-96-8)紅外圖譜(IR2)
InChI:InChI=1S/C9H12N2O6/c12-3-4-6(14)7(15)8(17-4)11-2-1-5(13)10-9(11)16/h1-2,4,6-8,12,14-15H,3H2,(H,10,13,16)/t4-,6-,7-,8-/m1/s1
InChIKey: DRTQHJPVMGBUCF-XVFCMESISA-N
Smiles:OC[C@H]1O[C@@H](N2C=CC(=O)NC2=O)[C@H](O)[C@@H]1O
400 MHz in D2O
400 MHz in DMSO-d6
-
| 1H NMR |
399.65 MHz |
| C9 H12 N2 O6
|
0.038 g : 0.5 ml D2O
|
| uridine
|
 |
Assign. Shift(ppm)
A 7.892
B 5.915
C 5.900
D 4.356
E 4.241
F 4.143
G *1 3.925
J *1 3.824
THE SOLVENT PEAK SUPPRESSED.
J(A,C)=8.0 HZ
J(B,D)=5.3 HZ
|
Hz ppm Int.
3158.08 7.903 553
3152.34 7.888 30
3150.02 7.882 569
2366.70 5.922 499
2362.18 5.911 1000
2354.00 5.891 481
1746.46 4.370 238
1741.21 4.357 395
1736.57 4.346 290
1700.44 4.255 257
1694.95 4.242 493
1689.58 4.228 271
1661.99 4.159 135
1659.06 4.152 180
1657.71 4.148 227
1654.79 4.141 201
1653.69 4.138 198
1652.34 4.135 180
1649.29 4.127 124
1578.25 3.950 182
1575.32 3.942 185
1565.43 3.918 321
1562.50 3.910 308
1535.40 3.842 306
1531.01 3.831 294
1522.58 3.810 189
1518.31 3.800 174
-
| 1H NMR |
399.65 MHz |
| C9 H12 N2 O6
|
0.039 g : 0.5 ml DMSO-d6
|
| uridine
|
|
Assign. Shift(ppm)
A 11.3
B 7.896
C 5.789
D 5.658
E 5.40
F 5.10
G 4.033
J 3.972
K 3.850
L *1 3.629
M *1 3.560
ASSIGNED BY H-H COSY.
J(B,D) = 8.1 HZ
J(C,G) = 5.5 HZ
|
Hz ppm Int.
4524.58 11.322 143
3159.99 7.907 971
3151.93 7.887 1000
2316.69 5.797 873
2311.19 5.784 879
2265.22 5.669 961
2257.16 5.648 954
2156.97 5.398 280
2153.85 5.390 247
2152.02 5.385 282
2151.66 5.384 282
2040.84 5.107 559
2036.26 5.096 415
1614.43 4.040 315
1609.67 4.028 345
1604.90 4.016 177
1590.62 3.981 291
1587.50 3.973 383
1583.29 3.962 231
1544.28 3.865 224
1541.16 3.857 583
1537.50 3.848 559
1534.20 3.839 211
1449.21 3.627 227
1448.30 3.624 219
1445.73 3.618 316
1445.37 3.617 317
1442.07 3.609 203
1430.16 3.579 213
1426.87 3.571 327
1423.57 3.563 216
1423.20 3.562 218