628-77-3

1,5-二碘戊烷(628-77-3)質(zhì)譜(MS)

產(chǎn)品名稱(chēng):1,5-二碘戊烷

CAS:628-77-3

分子式:C5H10I2

分子量: 323.94

InChI:InChI=1S/C5H10I2/c6-4-2-1-3-5-7/h1-5H2

InChIKey: IAEOYUUPFYJXHN-UHFFFAOYSA-N

Smiles:C(I)CCCCI

Mass

MS-NW-7288          
1,5-diiodopentane
C5H10I2             (Mass of molecular ion:    324)

   Source Temperature: 220 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      26.0       1.1
      27.0      16.2
      29.0       4.9
      38.0       1.6
      39.0      16.9
      40.0       3.3
      41.0      74.8
      42.0       9.9
      43.0       7.1
      53.0       3.0
      55.0       5.4
      67.0       2.5
      69.0      86.4
      70.0       6.8
     127.0       8.4
     128.0       4.7
     141.0       4.8
     154.0       1.3
     155.0      54.7
     156.0       1.3
     169.0       9.3
     197.0     100.0
     198.0       5.7
     211.0       1.1
     254.0       2.2
     324.0       8.8

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₅ H₁₀ I₂	0.05 ml : 0.5 ml CDCl₃
1,5-diiodopentane

    Assign.     Shift(ppm)

      A             3.194
      B             1.85
      C             1.54

     Hz     ppm     Int.

    292.88   3.271    374
    286.19   3.196   1000
    279.50   3.121    564
    181.50   2.027     70
    180.56   2.017     73
    173.69   1.940    246
    171.88   1.920    152
    167.06   1.866    405
    163.38   1.825    153
    160.38   1.791    355
    153.56   1.715    168
    150.50   1.681     89
    149.38   1.668     97
    148.81   1.662    100
    146.94   1.641    135
    143.88   1.607    140
    140.63   1.571    192
    139.25   1.555    126
    135.75   1.516    131
    135.44   1.513    131
    134.50   1.502    131
    133.19   1.488    132
    130.38   1.456     85
    129.19   1.443     69
    127.19   1.421     56
    126.75   1.416     57
    125.19   1.398     68

in CDCl3