62922-45-6

2,5-二氯戊胺鹽酸鹽(62922-45-6)核磁圖(¹HNMR)

產(chǎn)品名稱:2,5-二氯戊胺鹽酸鹽

CAS:62922-45-6

分子式:C5H12Cl3N

分子量: 192.51

Mass

MS-NW-9974          
2,5-dichloropentylamine hydrochloride
C5H11Cl2N HCl       (Mass of molecular ion:    155)

   Source Temperature: 160 °C
   Sample Temperature: 110 °C
   Direct, 75 eV

      18.0       3.2
      27.0       3.1
      28.0       4.8
      29.0       1.4
      30.0     100.0
      31.0       2.5
      35.0       1.5
      36.0      18.3
      38.0       6.0
      39.0       2.3
      41.0       2.9
      42.0       1.9
      43.0       1.5
      53.0       1.1
      56.0       2.4
     120.0       5.2
     122.0       1.6

400 MHz in DMSO-d6

¹H NMR	399.65 MHz
C₅ H₁₁ Cl₂ N	0.041 g : 0.5 ml DMSO-d₆
2,5-dichloropentylamine hydrochloride

    Assign.     Shift(ppm)

      A             8.6
      B             4.408
      C             3.690
      D     *1      3.26
      E     *1      3.06
      F             1.98
      G             1.83

     Hz     ppm     Int.

   3429.11   8.581    509
   1770.94   4.432    144
   1766.36   4.420    226
   1762.39   4.410    278
   1758.12   4.400    216
   1753.85   4.389    161
   1479.95   3.704    452
   1478.88   3.701    490
   1474.00   3.689   1000
   1467.90   3.673    521
   1308.90   3.276    136
   1296.39   3.244    176
   1226.81   3.070    128
   1220.55   3.055    157
   1211.55   3.032     96
    808.72   2.024    175
    807.19   2.020    237
    803.22   2.010    173
    799.26   2.000    200
    795.29   1.990    264
    793.30   1.985    191
    789.64   1.976    187
    788.42   1.973    186
    785.06   1.965    171
    781.86   1.957    179
    778.96   1.950    213
    775.45   1.941    206
    740.97   1.855    215
    739.29   1.850    236
    735.47   1.841    257
    731.81   1.832    310
    729.98   1.827    324
    726.47   1.818    271
    723.72   1.811    320
    722.35   1.808    311

in D2O

in DMSO-d6