1-氨基吡咯烷鹽酸鹽(63234-71-9)核磁圖(1HNMR)
InChI:InChI=1S/C4H10N2.ClH/c5-6-3-1-2-4-6;/h1-5H2;1H
InChIKey: KTVYGDJRKCXTRA-UHFFFAOYSA-N
Smiles:N1(N)CCCC1.[H]Cl
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Mass
MS-NW-6300
N-aminopyrrolidine hydrochloride
C4H10N2 HCl (Mass of molecular ion: 86)
Source Temperature: 260 °C
Sample Temperature: 190 °C
Reservoir, 75 eV
25.0 1.5
26.0 14.9
27.0 42.9
28.0 52.9
29.0 34.0
30.0 28.3
31.0 3.0
32.0 2.0
35.0 6.0
36.0 46.3
37.0 2.0
38.0 14.1
39.0 22.7
40.0 6.4
41.0 48.8
42.0 82.2
43.0 37.2
44.0 31.3
45.0 7.2
50.0 2.3
51.0 3.5
52.0 2.6
53.0 4.5
54.0 9.7
55.0 23.8
56.0 26.5
57.0 18.1
58.0 40.2
59.0 1.5
64.0 2.0
66.0 2.5
67.0 3.1
68.0 16.8
69.0 13.9
70.0 4.3
71.0 2.0
80.0 1.3
81.0 2.2
82.0 2.5
83.0 35.1
84.0 81.5
85.0 100.0
86.0 87.6
87.0 5.0
90 MHz in CDCl3
400 MHz in DMSO-d6
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| 1H NMR |
89.56 MHz |
| C4 H10 N2
|
0.042 g : 0.5 ml CDCl3
|
| N-aminopyrrolidine hydrochloride
|
 |
Assign. Shift(ppm)
A 7.5
B 3.57
C 2.13
|
Hz ppm Int.
675.94 7.548 376
327.06 3.652 291
320.00 3.574 816
313.06 3.496 368
198.13 2.213 352
194.25 2.169 414
191.00 2.133 1000
187.44 2.093 407
187.13 2.090 407
183.88 2.054 296
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| 1H NMR |
399.65 MHz |
| C4 H10 N2
|
0.040 g : 0.5 ml DMSO-d6
|
| N-aminopyrrolidine hydrochloride
|
|
Assign. Shift(ppm)
A 3.19
B 1.90
|
Hz ppm Int.
1274.54 3.190 359
760.25 1.903 1000