65016-55-9

3-癸基噻吩(65016-55-9)核磁圖(¹³CNMR)

產(chǎn)品名稱:3-癸基噻吩

CAS:65016-55-9

分子式:C14H24S

分子量: 224.41

InChI:InChI=1S/C14H24S/c1-2-3-4-5-6-7-8-9-10-14-11-12-15-13-14/h11-13H,2-10H2,1H3

InChIKey: JAYBIBLZTQMCAY-UHFFFAOYSA-N

Smiles:C1SC=CC=1CCCCCCCCCC

¹HNMR

¹³CNMR

IR1

Mass

MS-IW-3601          
3-decylthiophene
C14H24S             (Mass of molecular ion:    224)

   Source Temperature: 220 °C
   Sample Temperature: 160 °C
   Reservoir, 75 eV

      27.0       2.0
      29.0       3.5
      39.0       2.3
      41.0       6.6
      43.0       4.5
      45.0       3.9
      53.0       2.7
      55.0       2.8
      57.0       1.3
      67.0       1.2
      77.0       1.3
      84.0       1.3
      85.0       3.7
      97.0      46.7
      98.0     100.0
      99.0       9.8
     100.0       5.2
     110.0       1.4
     111.0      16.3
     112.0       2.0
     125.0       1.0
     139.0       1.9
     140.0       1.6
     224.0      14.3
     225.0       2.3

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₄ H₂₄ S	0.05 ml : 0.5 ml CDCl₃
3-decylthiophene

    Assign.     Shift(ppm)

      A             7.202
      B             6.915
      C             6.891
      D             2.607
      E             1.606
      F             1.32
      G             1.30
      J             1.28
      K             1.26
      L             0.879

     Hz     ppm     Int.

   2882.69   7.214    193
   2879.76   7.206    209
   2877.81   7.201    216
   2874.88   7.194    235
   2766.97   6.924    201
   2765.63   6.921    240
   2762.08   6.912    181
   2760.74   6.908    230
   2757.20   6.900    107
   2756.35   6.897    213
   2755.00   6.894    195
   2754.27   6.892    166
   2753.42   6.890    206
   2752.08   6.887    171
   2751.22   6.885     80
   1049.80   2.627    175
   1042.36   2.609    244
   1034.42   2.589    188
    649.90   1.627     83
    642.46   1.608    122
    635.01   1.589     96
    627.56   1.571     37
    519.90   1.301    357
    504.15   1.262   1000
    358.40   0.897    234
    351.56   0.880    729
    344.60   0.863    286

in CDCl3