6948-86-3

2,2′-甲基亞氨基雙(乙醛縮二乙醇)(6948-86-3)質(zhì)譜(MS)

產(chǎn)品名稱:2,2′-甲基亞氨基雙(乙醛縮二乙醇)

CAS:6948-86-3

分子式:C13H29NO4

分子量: 263.37

InChI:InChI=1S/C13H29NO4/c1-6-15-12(16-7-2)10-14(5)11-13(17-8-3)18-9-4/h12-13H,6-11H2,1-5H3

InChIKey: DPLOXPRJCFWURN-UHFFFAOYSA-N

Smiles:C(OCC)(OCC)CN(C)CC(OCC)OCC

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-5835          
N,N-bis(2,2-diethoxyethyl)methylamine
C13H29NO4           (Mass of molecular ion:    263)

   Source Temperature: 260 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      15.0       3.4
      18.0       1.8
      19.0       1.7
      26.0       1.7
      27.0       6.6
      28.0       3.8
      29.0      15.2
      30.0       1.3
      31.0      14.4
      41.0       1.9
      42.0      11.2
      43.0       6.8
      44.0      11.9
      45.0      10.5
      46.0       1.7
      47.0      33.1
      55.0       1.2
      56.0       1.4
      57.0       4.7
      58.0      14.9
      59.0      27.1
      60.0       1.5
      61.0      10.1
      70.0       3.1
      71.0       2.3
      72.0      11.0
      73.0       4.0
      74.0       1.0
      75.0      25.5
      76.0       1.0
      82.0       1.5
      84.0       2.9
      85.0       1.6
      86.0       4.9
      88.0       1.1
      89.0       5.0
      96.0       1.6
      97.0       1.2
      98.0       2.1
      99.0       1.1
     100.0       3.9
     101.0       4.1
     102.0       6.5
     103.0      30.9
     104.0       1.8
     114.0      31.7
     115.0       2.9
     116.0      28.5
     117.0       2.8
     125.0       1.2
     129.0       2.6
     130.0       2.1
     132.0       2.6
     142.0       1.1
     146.0      13.8
     147.0       3.7
     158.0       2.6
     160.0     100.0
     161.0       8.7
     171.0       1.6
     172.0      16.0
     173.0       2.3
     174.0       1.1
     204.0       3.0
     217.0       4.3
     218.0      13.0
     219.0       3.1

90 MHz in CDCl3

¹H NMR	89.56 MHz
C₁₃ H₂₉ N O₄	0.04 ml : 0.5 ml CDCl₃
N,N-bis(2,2-diethoxyethyl)methylamine

    Assign.     Shift(ppm)

      A             4.608
      B     *1      3.659
      C     *1      3.526
      D             2.652
      E             2.408
      F             1.212
     
     J(A,D)=5.2HZ. J(B,F)=J(C,F)=7.0HZ. J(B,C)=9.3HZ.

     Hz     ppm     Int.

    418.38   4.672     56
    413.13   4.613    133
    407.88   4.555     75
    339.19   3.788     48
    337.06   3.764     59
    332.06   3.708     60
    331.13   3.698     68
    329.88   3.684    181
    324.06   3.619    180
    322.75   3.604    199
    317.13   3.541    179
    315.69   3.525     84
    314.75   3.515     56
    310.19   3.464     67
    307.75   3.437     49
    240.13   2.682    208
    234.88   2.623    196
    215.63   2.408    321
    115.38   1.289    450
    108.31   1.210   1000
    101.25   1.131    386

in CDCl3

liquid film

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2,2′-甲基亞氨基雙(乙醛縮二乙醇)(6948-86-3)質(zhì)譜(MS)