707-61-9

3-甲基-1-苯基-2-磷 1-氧化物(707-61-9)核磁圖(¹HNMR)

產(chǎn)品名稱:3-甲基-1-苯基-2-磷 1-氧化物

CAS:707-61-9

分子式:C11H13OP

分子量: 192.19

InChI:InChI=1S/C11H13OP/c1-10-7-8-13(12,9-10)11-5-3-2-4-6-11/h2-6,9H,7-8H2,1H3

InChIKey: YMKWWHFRGALXLE-UHFFFAOYSA-N

Smiles:P1(=O)(C2=CC=CC=C2)C=C(C)CC1

¹HNMR

¹³CNMR

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₁ H₁₃ O P	0.042 g : 0.5 ml CDCl₃
3-methyl-1-phenyl-2-phospholene 1-oxide

    Assign.     Shift(ppm)

      A             7.69
      B             7.49
      C             5.945
      D     *1      2.83
      E     *1      2.63
      F             2.23
      G             2.083

     Hz     ppm     Int.

   3085.82   7.722     35
   3084.11   7.718     49
   3081.79   7.712    147
   3080.44   7.708    187
   3073.97   7.692    214
   3072.27   7.688    216
   3069.58   7.681    167
   3068.24   7.678    200
   3061.77   7.662    209
   3060.18   7.658    191
   3011.60   7.536     47
   3010.25   7.533     58
   3008.79   7.529     52
   3007.57   7.526     47
   3004.15   7.517    140
   3002.81   7.514    151
   2999.02   7.505    136
   2997.44   7.501    244
   2995.85   7.497    251
   2993.41   7.491    289
   2990.72   7.484    274
   2985.60   7.471    275
   2983.52   7.466    257
   2979.61   7.456     97
   2977.42   7.451     97
   2974.85   7.444     57
   2389.40   5.979    134
   2388.18   5.976    135
   2364.38   5.917    135
   2363.04   5.913    134
   1147.71   2.872     42
   1146.97   2.870     41
   1142.58   2.859     47
   1142.21   2.859     47
   1137.82   2.848     55
   1134.64   2.840     44
   1130.37   2.829     72
   1124.51   2.814     66
   1116.58   2.794     34
   1116.21   2.793     34
   1064.82   2.665     49
   1063.84   2.662     46
   1062.74   2.660     45
   1061.89   2.658     44
   1059.08   2.651     58
   1058.35   2.649     59
   1057.74   2.647     60
   1057.50   2.647     60
   1054.93   2.640     54
   1054.32   2.639     54
   1053.34   2.636     56
   1052.86   2.635     55
   1051.76   2.632     54
   1047.85   2.622     56
   1047.49   2.622     55
   1042.97   2.610     36
   1040.89   2.605     39
   1040.65   2.604     39
   1039.92   2.603     39
    907.71   2.272     69
    903.08   2.260     74
    898.44   2.249    109
    893.68   2.237    133
    891.97   2.232    121
    889.40   2.226    148
    886.47   2.219    119
    884.28   2.213    196
    881.23   2.206    102
    878.42   2.198     91
    876.22   2.193     78
    873.90   2.187     37
    832.76   2.084   1000

in CDCl3