73579-08-5

1-甲基-4-(甲氨基)哌啶(73579-08-5)質譜(MS)

產(chǎn)品名稱:1-甲基-4-(甲氨基)哌啶

CAS:73579-08-5

分子式:C7H16N2

分子量: 128.22

¹HNMR

¹³CNMR

IR1

Mass

MS-NW-9662          
N(4),1-dimethyl-4-piperidinamine
C7H16N2             (Mass of molecular ion:    128)

   Source Temperature: 270 °C
   Sample Temperature: 150 °C
   Reservoir, 75 eV

      15.0       3.0
      18.0       1.5
      27.0       4.1
      28.0       7.6
      29.0       4.2
      30.0       6.0
      39.0       3.4
      41.0       6.5
      42.0      38.4
      43.0      59.1
      44.0      29.9
      45.0       1.0
      52.0       1.0
      53.0       2.0
      54.0       4.4
      55.0      13.2
      56.0      14.3
      57.0      12.7
      58.0      11.2
      67.0       1.2
      68.0       8.6
      69.0       4.4
      70.0      34.3
      71.0      17.7
      72.0       2.2
      79.0       1.1
      80.0       1.0
      81.0       1.8
      82.0      27.3
      83.0       2.3
      84.0       6.5
      85.0       3.4
      94.0       2.6
      96.0      64.1
      97.0     100.0
      98.0      12.8
      99.0       3.7
     128.0       4.5
     129.0       1.3

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₇ H₁₆ N₂	0.05 ml : 0.5 ml CDCl₃
N(4),1-dimethyl-4-piperidinamine

    Assign.     Shift(ppm)

      A             2.805
      B             2.427
      C             2.329
      D             2.263
      E             1.987
      F             1.873
      G             1.379
      J             1.23
     
     ASSIGNED BY H-H COSY.

     Hz     ppm     Int.

   1127.20   2.821     83
   1118.16   2.798     61
   1115.11   2.791     90
    969.97   2.428   1000
    942.14   2.358     35
    935.79   2.342     40
    931.76   2.332     68
    927.73   2.322     44
    925.54   2.316     32
    921.39   2.306     38
    908.45   2.274     68
    904.42   2.264    950
    807.13   2.020     55
    804.81   2.014     63
    795.41   1.991    102
    793.21   1.985    116
    783.81   1.962     56
    781.62   1.956     64
    757.69   1.896     67
    756.84   1.894     72
    755.49   1.891     77
    754.15   1.888     73
    752.93   1.884     71
    749.02   1.875     49
    745.12   1.865     75
    744.02   1.862     81
    742.55   1.859     86
    741.33   1.855     80
    740.36   1.853     77
    569.82   1.426     39
    566.04   1.417     40
    558.35   1.398     67
    557.01   1.394     72
    555.66   1.391     71
    554.57   1.388     75
    546.63   1.368     67
    545.65   1.366     65
    544.19   1.362     66
    542.72   1.358     63
    535.03   1.339     30
    531.25   1.330     30

in CDCl3