90-15-3

1-萘酚(90-15-3)質(zhì)譜(MS)

產(chǎn)品名稱:1-萘酚

CAS:90-15-3

分子式:C10H8O

分子量: 144.17

InChI:InChI=1S/C10H8O/c11-10-7-3-5-8-4-1-2-6-9(8)10/h1-7,11H

InChIKey: KJCVRFUGPWSIIH-UHFFFAOYSA-N

Smiles:C1(O)=C2C(C=CC=C2)=CC=C1

Mass

MS-NW-6154          
1-naphthol
C10H8O              (Mass of molecular ion:    144)

   Source Temperature: 250 °C
   Sample Temperature: 190 °C
   Reservoir, 75 eV

      38.0       1.2
      39.0       3.8
      50.0       2.4
      51.0       2.7
      57.0       3.7
      57.5       4.7
      58.0       5.6
      61.0       1.1
      62.0       3.0
      63.0       6.3
      64.0       1.3
      65.0       2.7
      72.0       5.9
      74.0       2.2
      75.0       1.9
      77.0       1.0
      86.0       1.3
      87.0       1.8
      88.0       1.7
      89.0       6.0
      90.0       1.3
     113.0       1.6
     114.0       2.8
     115.0      56.1
     116.0      30.6
     117.0       2.9
     143.0       1.5
     144.0     100.0
     145.0      11.3

400 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₀ H₈ O	0.039 g : 0.5 ml CDCl₃
1-naphthol

    Assign.     Shift(ppm)

      A             8.161
      B             7.786
      C             7.47
      D             7.45
      E             7.417
      F             7.259
      G             6.734
      J             5.43

     Hz     ppm     Int.

   3269.41   8.181     74
   3268.55   8.179     90
   3267.21   8.176    254
   3266.48   8.174    403
   3265.75   8.172    283
   3265.14   8.171    251
   3264.16   8.168    214
   3262.08   8.163    198
   3261.23   8.161    342
   3260.62   8.159    279
   3259.77   8.157    253
   3259.03   8.155    242
   3257.57   8.152    274
   3256.84   8.150    422
   3256.10   8.148    249
   3120.85   7.809     78
   3120.48   7.809     79
   3117.31   7.801    389
   3114.99   7.795    298
   3113.16   7.790    376
   3109.74   7.782    284
   3109.38   7.781    296
   3107.79   7.777    439
   3105.35   7.771     79
   2992.80   7.489     95
   2990.60   7.484    231
   2985.96   7.472    804
   2984.74   7.469    832
   2983.76   7.466    665
   2980.83   7.459    917
   2980.35   7.458    867
   2977.17   7.450    654
   2976.44   7.448    724
   2975.10   7.445    701
   2973.51   7.441    111
   2970.21   7.433    473
   2969.24   7.430    579
   2961.91   7.412    428
   2960.94   7.409    700
   2960.57   7.408    649
   2908.57   7.278    759
   2901.12   7.260    880
   2900.39   7.258    661
   2892.94   7.239    615
   2695.56   6.745    761
   2694.58   6.743    736
   2688.11   6.727    707
   2687.13   6.724    674
   2170.53   5.432   1000

in CDCl3