91-63-4

2-甲基喹啉(91-63-4)紅外圖譜(IR2)

產品名稱:2-甲基喹啉

CAS:91-63-4

分子式:C10H9N

分子量: 143.19

InChI:InChI=1S/C10H9N/c1-8-6-7-9-4-2-3-5-10(9)11-8/h2-7H,1H3

InChIKey: SMUQFGGVLNAIOZ-UHFFFAOYSA-N

Smiles:N1C2C(=CC=CC=2)C=CC=1C

Mass

MS-NW-0146          
2-methylquinoline
C10H9N              (Mass of molecular ion:    143)

   Source Temperature: 200 °C
   Sample Temperature:  75 °C
   Reservoir, 75 eV

      27.0       1.3
      28.0       1.1
      38.0       1.3
      39.0       4.4
      50.0       5.1
      51.0       6.5
      52.0       1.8
      57.5       1.1
      58.5       3.6
      62.0       2.0
      63.0       4.8
      64.0       1.3
      65.0       1.3
      70.5       1.9
      71.5       3.9
      74.0       2.8
      75.0       5.5
      76.0       4.9
      77.0       4.4
      87.0       1.0
      88.0       1.0
      89.0       3.7
      90.0       2.1
     101.0       5.9
     102.0       3.3
     103.0       1.1
     113.0       1.0
     114.0       1.3
     115.0      14.4
     116.0       6.6
     117.0       3.5
     128.0      14.6
     129.0       2.4
     140.0       2.2
     141.0       1.4
     142.0      11.2
     143.0     100.0
     144.0      11.3

400 MHz in CDCl3

90 MHz in CDCl3

¹H NMR	399.65 MHz
C₁₀ H₉ N	24.5 mg : 0.5 ml CDCl₃
2-methylquinoline

    Assign.     Shift(ppm)

      A             8.03
      B             7.759
      C             7.677
      D             7.475
      E             7.271
      F             2.745

     Hz     ppm     Int.

   3213.26   8.041    203
   3212.77   8.039    202
   3204.96   8.020    224
   3204.47   8.019    218
   3106.20   7.773     71
   3104.49   7.769     82
   3097.78   7.752     86
   3096.31   7.748     88
   3076.66   7.699     48
   3075.32   7.696     44
   3069.82   7.682     57
   3068.36   7.678    103
   3067.02   7.675     44
   3061.40   7.661     48
   3060.06   7.657     51
   2994.75   7.494     58
   2993.77   7.491     55
   2987.79   7.477     55
   2986.69   7.474     94
   2985.47   7.471     55
   2979.74   7.456     42
   2978.52   7.453     41
   2909.79   7.281    151
   2901.37   7.260    138
   1097.29   2.746   1000

¹H NMR	89.56 MHz
C₁₀ H₉ N	0.024 g : 0.5 ml CDCl₃
2-methylquinoline

    Assign.     Shift(ppm)

      A             8.02
      B             7.75
      C             7.67
      D             7.47
      E             7.265
      F             2.739

     Hz     ppm     Int.

    722.50   8.068    147
    714.19   7.975    195
    699.50   7.811     41
    697.81   7.792     46
    695.19   7.763     41
    693.13   7.740     47
    690.13   7.706     97
    687.88   7.681     98
    686.88   7.670     40
    686.25   7.663     37
    680.00   7.593     67
    678.38   7.575     37
    675.06   7.538     75
    673.69   7.523     72
    667.88   7.458     61
    666.75   7.445     53
    666.00   7.437     38
    654.25   7.306    161
    645.88   7.212    116
    245.38   2.740   1000

in CDCl3