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Journal of pharmaceutical sciences

Journal of pharmaceutical sciences

IF: 3.7
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2-(Methylamino)-5-chlorobenzophenone Imine: A Novel Product Formed in Base-Catalyzed Hydrolysis of Diazepam

Published:1 July 1996 DOI: 10.1021/js9504245 PMID: 8819000
Shen K. Yang, Ren Tang, Tian Jian Yang, Quan-Long Pu, Ziping Bao

Abstract

Diazepam (1), a hypnotic and anxiolytic drug in worldwide use, formed an intermediate product in a mixture of ethanol and sodium hydroxide ([NaOH] ≥ 1 M). The intermediate product slowly decomposed to form 2-(methylamino)-5-chlorobenzophenone imine (2) and 2-(methyl-amino)-5-chlorobenzophenone (3). The amount of 2 formed, relative to that of 3, increased with increasing NaOH concentration. Compound 2, a heretofore unknown derivative of 1, was characterized by high-performance liquid chromatography, ultraviolet–visible absorption, mass, and proton nuclear magnetic resonance spectral analyses.

Substances (5)

Related products
Procduct Name CAS Molecular Formula Supplier Price
Sodium hydroxide 1310-73-2 NaOH 1358 suppliers $14.00-$17490.00
Ethanol 64-17-5 C2H6O 955 suppliers $10.00-$28350.00
5-Chloro-2-(methylamino)benzophenone 1022-13-5 C14H12ClNO 366 suppliers $10.00-$1390.00
N,3-diMethyl-5-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)pyridin-2-aMine 1111637-92-3 C13H21BN2O2 38 suppliers $89.65-$5520.00
2-(methylamino)-5-chlorobenzophenone imine 5606-40-6 C14H13ClN2 14 suppliers Inquiry

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