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1,1,5-TRIACETOXY-2,2-DICHLOROPENTANE, 97 synthesis

2synthesis methods

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 92 percent / NaOAc, Ac₂O / 1 h / 110 - 120 °C
2: 84.6 percent / conc. H₂SO₄, Ac₂O / 46.5 h / 135 °C

References:

Buyck, Laurent de;Vanhulle, Peter [Bulletin des Societes Chimiques Belges,1992,vol. 101,# 4,p. 329 - 336]

64-19-7 Synthesis

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