1,1'-Carbonyldiimidazole synthesis
- Product Name:1,1'-Carbonyldiimidazole
- CAS Number:530-62-1
- Molecular formula:C7H6N4O
- Molecular Weight:162.15
DOI: 10.15227/orgsyn.048.0044
32315-10-9
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530-62-1
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Yield:530-62-1 90.5%
Reaction Conditions:
in dichloromethane at 26; for 0.5 h;Inert atmosphere;Temperature;
Steps:
1.2; 1.3; 2.2; 2.3; 3.2; 3.3; 4.2; 4.3
Add 0.04 mol of triphosgene and 200 ml of dichloromethane to a three-necked flask.Stir until the phosgene dissolves,Cool the mixture to 26 ° C,Under nitrogen protection conditions,To the mixture, N-trimethylsilazole 0.28 mol was added dropwise.The dropping time is 30 min, that is, the product carbonyl diimidazole reaction liquid is obtained;(3) The carbonyl diimidazole reaction liquid prepared in the step (2) is filtered, and the filtered product is subjected to vacuum drying at a temperature of 72 ° C to obtain a powdery carbonyl diimidazole.
References:
CN109232430,2019,A Location in patent:Paragraph 0015; 0017; 0019; 0021; 0023; 0025; 0027-0032
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32315-10-9
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$10.00/1g
530-62-1
966 suppliers
$6.00/25g
288-32-4
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