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ChemicalBook CAS DataBase List 1,1'-DIBROMOFERROCENE
1293-65-8

1,1'-DIBROMOFERROCENE synthesis

4synthesis methods
-

Yield:1293-65-8 89%

Reaction Conditions:

Stage #1:ferrocene with n-butyllithium;N,N,N,N,-tetramethylethylenediamine in hexane at 20;Inert atmosphere;
Stage #2: with 1,2-dibromo-1,1,2,2-tetrachloroethane in tetrahydrofuran;dichloromethane at -78 - 20; for 5 h;Inert atmosphere;

References:

Khobragade, Dushant A.;Mahamulkar, Shraddha G.;Pospí?il, Lubomír;Císa?ová, Ivana;Rulí?ek, Lubomír;Jahn, Ullrich [Chemistry - A European Journal,2012,vol. 18,# 39,p. 12267 - 12277] Location in patent:supporting information

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