1-(2,6-dichlorophenyl)propan-1-ol synthesis
3synthesis methods
- Product Name:1-(2,6-dichlorophenyl)propan-1-ol
- CAS Number:835925-30-9
- Molecular formula:C9H10Cl2O
- Molecular Weight:205.0811
Yield:835925-30-9 92%
Reaction Conditions:
Stage #1: ethyl iodidewith 1-butylpyridinium bromide;N-butylpyridinium tetrafluoroborate;zinc at 50; for 1 h;
Stage #2: 2,6-dichlorobenzaldehyde at 50; for 12 h;
References:
Law, Man Chun;Wong, Kwok-Yin;Chan, Tak Hang [Journal of Organic Chemistry,2005,vol. 70,# 25,p. 10434 - 10439]