ChemicalBook CAS DataBase List 1,2-Dichloropropane

1,2-Dichloropropane synthesis

12synthesis methods

Product Name:1,2-Dichloropropane
CAS Number:78-87-5
Molecular formula:C3H6Cl2
Molecular Weight:112.99

187737-37-7 Synthesis

187737-37-7
1 suppliers
inquiry

78-87-5
268 suppliers
$14.00/25g

75-29-6 Synthesis

75-29-6
316 suppliers
$20.00/25mL

67-63-0 Synthesis

67-63-0
1670 suppliers
$17.00/25ML

67-64-1
0 suppliers
$19.10/10ml

Yield:67-63-0 1087 μmol ，75-29-6 80.1 μmol ，67-64-1 18.8 μmol ，78-87-5 15.6 μmol

Reaction Conditions:

with copper(l) chloride;sodium chloride;copper dichloride at 150; for 0.25 h;Reagent/catalyst;Temperature;

Steps:

1; 2; 6; 7 Experiment 2:

A solution of CuCl₂(0.71 mol/kg), CuCl (0.71 mol/kg), and NaCl (2.76 mol/kg) was heated in a Parr reactor under propylene pressure to 150°C for 15 minutes. The reactor was depressurized into a bubbler trap at 0°C to capture volatile compounds. When the reactor was opened, the solution was extracted three times with an organic solvent, e.g. ethyl acetate or dichloromethane, which was analyzed with a gas chromatograph equipped with a mass spectrometer. A total of 15.6 umol DCP and 62.4 umol PCH were measured. The amounts of recyclable products measured were 1087 umol isopropanol, 18.8 umol acetone, and 80.1 umol isopropyl chloride.

References:

WO2018/222642,2018,A1 Location in patent:Paragraph 161-163; 168; 169

187737-37-7 Synthesis

187737-37-7
1 suppliers
inquiry

78-87-5
268 suppliers
$14.00/25g

References

56-81-5 Synthesis