1,2-Dimethylisothiourea hydriodate synthesis
1synthesis methods
- Product Name:1,2-Dimethylisothiourea hydriodate
- CAS Number:41306-45-0
- Molecular formula:C3H9IN2S
- Molecular Weight:232.09
MeI (17.0 g, 120 mmol) was added to N-methylthiourea (100 mmol) in an anhydrous EtOH (100 )
mL) in a suspension of N-methylthiourea, exothermic dissolution of the thiourea occurred, indicating that the reaction was underway. The completion of the reaction
Yield: 100%
Reaction Conditions:
in methanol for 1 h;
References:
Larsen;Connell;Cudahy;Evans;May;Meglasson;O'Sullivan;Schostarez;Sih;Stevens;Tanis;Tegley;Tucker;Vaillancourt;Vidmar;Watt;Yu [Journal of Medicinal Chemistry,2001,vol. 44,# 8,p. 1217 - 1230]