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ChemicalBook CAS DataBase List 1,4-BENZENEDIMETHANETHIOL
105-09-9

1,4-BENZENEDIMETHANETHIOL synthesis

4synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 3 steps
1: dibenzoyl peroxide; bromine / tetrachloromethane / 5.33 h / Reflux; UV-irradiation
2: acetone / 1 h / Reflux
3: sodium hydroxide; hydrogenchloride; water / 3 h / pH Ca.2 / Reflux

References:

Ostasz;Lyszczek;Mazur;Tarasiuk [CrystEngComm,2014,vol. 16,# 44,p. 10262 - 10272]

FullText

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