1-[4-Methoxy-2-(methoxymethoxy)phenyl]ethanone synthesis
- Product Name:1-[4-Methoxy-2-(methoxymethoxy)phenyl]ethanone
- CAS Number:58544-83-5
- Molecular formula:C11H14O4
- Molecular Weight:210.23
552-41-0
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$5.00/1g
107-30-2
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$110.00/2.5g
58544-83-5
12 suppliers
$180.25/1gm:
Yield:58544-83-5 70%
Reaction Conditions:
Stage #1: 1-(2-hydroxy-4-methoxyphenyl)ethanonewith sodium hydride in tetrahydrofuran;mineral oil at 0; for 0.5 h;
Stage #2: chloromethyl methyl ether in tetrahydrofuran;mineral oil at 20; for 16 h;
References:
Kobayashi, Toshitake;Sasaki, Satoshi;Tomita, Naoki;Fukui, Seiji;Kuroda, Noritaka;Nakayama, Masaharu;Kiba, Atsushi;Takatsu, Yoshihiro;Ohtaki, Tetsuya;Itoh, Fumio;Baba, Atsuo [Bioorganic and Medicinal Chemistry,2010,vol. 18,# 11,p. 3841 - 3859] Location in patent:experimental part