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ChemicalBook CAS DataBase List 1-Chloro-2-butene
591-97-9

1-Chloro-2-butene synthesis

9synthesis methods
pure isomers of 1-Chloro-2-butene can be prepared by chloride displacement of corresponding alcohols via Ph3P in various solvents, and other chlorinating agents.
-

Yield:591-97-9 70 %Spectr.

Reaction Conditions:

with oxalyl dichloride;Triphenylphosphine oxide in chloroform at 20; for 7 h;

References:

Denton, Ross M.;An, Jie;Adeniran, Beatrice [Chemical Communications,2010,vol. 46,# 17,p. 3025 - 3027] Location in patent:supporting information; experimental part

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