1-Nitro-3-oxiranylbenzene synthesis
- Product Name:1-Nitro-3-oxiranylbenzene
- CAS Number:20697-05-6
- Molecular formula:C8H7NO3
- Molecular Weight:165.15
586-39-0
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20697-05-6
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Yield:20697-05-6 93%
Reaction Conditions:
with dihydrogen peroxide;N,N-dimethyl-formamide in water at 100; for 2 h;Green chemistry;
Steps:
General procedure: Styrene (0.10 g, 1.00 mmol) was added to a round-bottomedflask containing colloidal of Pd(II)AEA-Fe3O4NP(0.1 g) and DMA (0.02 mmol) in H2O (5 mL) and temperatureraise up to 100 °C. H2O2 (3 mmol) was addeddropwise to the reaction vessel during 0.5 h. After 1.5 h,the reaction mixture was cooled to room temperature, andPd(II)AEA-Fe3O4NP was separated by a magnet andwashed with acetone (2 × 5 mL). The filtrate solvent wasevaporated under vacuum, and the product purified withcolumn chromatography with n-hexane/ethylacetate (5:1).
References:
Keshipour, Sajjad;Khalteh, Nastaran Kalam [Journal of the Iranian Chemical Society,2016,vol. 13,# 11,p. 1977 - 1982]
2227-64-7
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13425-36-0
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20697-05-6
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