2,7-Dihydroxy-3,6,10,11-tetrakis(pentyloxy)triphenylene synthesis
- Product Name:2,7-Dihydroxy-3,6,10,11-tetrakis(pentyloxy)triphenylene
- CAS Number:102737-76-8
- Molecular formula:C38H52O6
- Molecular Weight:604.82
110-53-2
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: potassium carbonate / ethanol; acetone / 24 h / Inert atmosphere; Reflux
2: iron(III) chloride; sulfuric acid / dichloromethane / 1.5 h
3: diphenylphosphane; n-butyllithium / tetrahydrofuran; hexane / 20 - 60 °C / Inert atmosphere
References:
Bi, Jingze;Wu, Hao;Zhang, Zhenhu;Zhang, Ao;Yang, Huanzhi;Feng, Yuwen;Fang, Yi;Zhang, Lina;Wang, Zhengran;Qu, Wentao;Liu, Feng;Zhang, Chunxiu [Journal of Materials Chemistry C,2019,vol. 7,# 40,p. 12463 - 12469]
120-80-9
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909119-73-9
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102737-76-8
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142947-21-5
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102737-76-8
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