1,5-Benzothiazepin-4(5H)-one, 2,3-dihydro-7-methoxy- synthesis

3synthesis methods

Product Name:1,5-Benzothiazepin-4(5H)-one, 2,3-dihydro-7-methoxy-
CAS Number:110766-87-5
Molecular formula:C10H11NO2S
Molecular Weight:209.26

696-63-9 Synthesis

696-63-9
190 suppliers
$10.00/1g

1,5-Benzothiazepin-4(5H)-one, 2,3-dihydro-7-methoxy-

110766-87-5
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Yield:-

Steps:

Multi-step reaction with 4 steps
1: borax / water / 20 °C
2: sodium hydroxide / methanol / 20 °C
3: trifluoroacetic acid; trifluoroacetic anhydride / 60 °C
4: trifluoroacetic acid; trimethylsilylazide / 48 h / 20 °C

References:

Smith, Chris D.;Wang, Aixia;Vembaiyan, Kannan;Zhang, Jingqun;Xie, Cuihong;Zhou, Qiang;Wu, Guogen;Chen, S. R. Wayne;Back, Thomas G. [Journal of Medicinal Chemistry,2013,vol. 56,# 21,p. 8626 - 8655]

13739-36-1 Synthesis

13739-36-1
33 suppliers
$45.00/25mg

110766-87-5
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References

57-57-8
178 suppliers
$24.73/250mgs:

14482-32-7
18 suppliers
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110766-87-5
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References

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1,5-Benzothiazepin-4(5H)-one, 2,3-dihydro-7-methoxy- synthesis