4-(TRIFLUOROMETHYL)UMBELLIFERYL-BETA-D-GLUCOPYRANOSIDE synthesis

1synthesis methods

Product Name:4-(TRIFLUOROMETHYL)UMBELLIFERYL-BETA-D-GLUCOPYRANOSIDE
CAS Number:116981-86-3
Molecular formula:C16H15F3O8
Molecular Weight:392.28

575-03-1 Synthesis

575-03-1
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2,3,4,6-Tetra-O-acetyl-alpha-D-glucopyranosyl bromide

572-09-8
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4-(TRIFLUOROMETHYL)UMBELLIFERYL-BETA-D-GLUCOPYRANOSIDE

116981-86-3
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Yield:-

Steps:

Multi-step reaction with 2 steps
1: silver(l) oxide; 2,6-dimethylpyridine / acetonitrile / 17 h / Inert atmosphere; Molecular sieve
2: sodium methylate / methanol / Inert atmosphere

References:

Danby, Phillip M.;Withers, Stephen G. [Journal of the American Chemical Society,2017,vol. 139,# 31,p. 10629 - 10632]

4-(TRIFLUOROMETHYL)UMBELLIFERYL-BETA-D-GLUCOPYRANOSIDE Related Search:

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4-(TRIFLUOROMETHYL)UMBELLIFERYL-BETA-D-GLUCOPYRANOSIDE synthesis

4-(TRIFLUOROMETHYL)UMBELLIFERYL-BETA-D-GLUCOPYRANOSIDE Related Search: