2,2'-((2,5-di(pyridin-4-yl)-1,4-phenylene)bis(oxy))diethanol synthesis
1synthesis methods
- Product Name:2,2'-((2,5-di(pyridin-4-yl)-1,4-phenylene)bis(oxy))diethanol
- CAS Number:1186466-82-9
- Molecular formula:C20H20N2O4
- Molecular Weight:352.38
Yield:1186466-82-9 88%
Reaction Conditions:
with tetrakis(triphenylphosphine) palladium(0);potassium carbonate in ethanol;water;toluene at 90; for 40 h;Schlenk technique;Inert atmosphere;
References:
Zhang, Zeyuan;Zhao, Zhengqing;Hou, Yali;Wang, Heng;Li, Xiaopeng;He, Gang;Zhang, Mingming [Angewandte Chemie - International Edition,2019,vol. 58,# 26,p. 8862 - 8866][Angew. Chem.,2019,vol. 131,# 26,p. 8954 - 8958,5] Location in patent:supporting information