1,3,2-DIOXABOROLANE, 2-(3,5-DIMETHOXY-4-METHYLPHENYL)-4,4,5,5-TETRAMETHYL- synthesis
- Product Name:1,3,2-DIOXABOROLANE, 2-(3,5-DIMETHOXY-4-METHYLPHENYL)-4,4,5,5-TETRAMETHYL-
- CAS Number:1345024-09-0
- Molecular formula:C15H23BO4
- Molecular Weight:278.15
5673-07-4
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1345024-09-0
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Yield:1345024-09-0 93%
Reaction Conditions:
Stage #1: bis(pinacol)diboranewith (1,5-cyclooctadiene)(methoxy)iridium(I) dimer;4,4'-di-tert-butyl-2,2'-bipyridine in octane at 20; for 0.25 h;
Stage #2: 2,6-dimethoxytoluene in octane at 125; for 72 h;
References:
Schwaben, Jonas;Cordes, Jens;Harms, Klaus;Koert, Ulrich [Synthesis,2011,# 18,art. no. T64711SS,p. 2929 - 2934] Location in patent:experimental part