5-CHLORO-1,3-DIHYDRO-2H-PYRROLO[3,2-B] PYRIDIN-2-ONE synthesis
- Product Name:5-CHLORO-1,3-DIHYDRO-2H-PYRROLO[3,2-B] PYRIDIN-2-ONE
- CAS Number:136888-08-9
- Molecular formula:C7H5ClN2O
- Molecular Weight:168.58
16013-85-7
504 suppliers
$9.00/5g
136888-08-9
98 suppliers
$177.47/250mg
Yield:-
Steps:
Multi-step reaction with 2 steps
1.1: sodium hydride / 1,2-dimethoxyethane / 2 h / 20 °C
1.2: 18 h / 20 °C
2.1: hydrogen / ethanol; water / 48 h / 2280.15 Torr
2.2: 5 h / Reflux
References:
Hoffmann-La Roche Inc.;Alam, Muzaffar;Du Bois, Daisy Jo;Hawley, Ronald Charles;Minatti, Ana Elena;Kennedy-Smith, Joshua;Thakkar, Kshitij Chhabilbhai;Wilhelm, Robert Stephen US2013/158066, 2013, A1
16013-85-7
504 suppliers
$9.00/5g
105-53-3
808 suppliers
$5.00/25g
136888-08-9
98 suppliers
$177.47/250mg