2,3,3a,6,7,7a-Hexahydro-2S,7a-diMethyl-4-hydroxy-indene-1R-(1'-iodo)ethane 4-O-TrifluoroMethylsulfonate synthesis

3synthesis methods

Product Name:2,3,3a,6,7,7a-Hexahydro-2S,7a-diMethyl-4-hydroxy-indene-1R-(1'-iodo)ethane 4-O-TrifluoroMethylsulfonate
CAS Number:145372-33-4
Molecular formula:C14H20F3IO3S
Molecular Weight:452.27

37595-74-7 Synthesis

Yield:145372-33-4 92%

Reaction Conditions:

with lithium diisopropyl amide in tetrahydrofuran at -78; for 2 h;

References:

Sestelo, Jose Perez;Mascarenas, Jose L.;Castedo, Luis;Murino, Antonio [Journal of Organic Chemistry,1993,vol. 58,# 1,p. 118 - 123]

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