Butanethioic acid, S1,S1',S1'',S1''',S1'''',S1'''''-(2,3,6,7,10,11-triphenylenehexayl) ester synthesis
- Product Name:Butanethioic acid, S1,S1',S1'',S1''',S1'''',S1'''''-(2,3,6,7,10,11-triphenylenehexayl) ester
- CAS Number:1586745-04-1
- Molecular formula:C42H48O6S6
- Molecular Weight:841.22
![2,3,6,7,10,11-hexabromobenzo[9,10]phenanthrene](/CAS/GIF/82632-80-2.gif)
82632-80-2
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1586745-04-1
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Yield:1586745-04-1 67%
Reaction Conditions:
Stage #1: 2,3,6,7,10,11-hexabromo-triphenylenewith 1,3-dimethyl-2-imidazolidinone;sodium thiomethoxide at 240; for 48 h;Schlenk technique;Inert atmosphere;
Stage #2: butyryl chloride at 0; for 2 h;Schlenk technique;Inert atmosphere;
References:
Huang, Jiahong;He, Yonghe;Yao, Ming-Shui;He, Jun;Xu, Gang;Zeller, Matthias;Xu, Zhengtao [Journal of Materials Chemistry A,2017,vol. 5,# 31,p. 16139 - 16143] Location in patent:supporting information