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ChemicalBook CAS DataBase List 17-IODOHEPTADECANOIC ACID
60451-92-5

17-IODOHEPTADECANOIC ACID synthesis

9synthesis methods
-

Yield:-

Steps:

Multi-step reaction with 7 steps
1: NH3 / tetrahydrofuran / 15 h
2: diethyl ether
3: LiAlH4 / diethyl ether / 2 h / 0 °C
4: 54 percent / LiNH2, Fe(NO3)3 / tetrahydrofuran; NH3 / 20 h
5: H2 / PtO2 / diethyl ether
6: pyridine / 0 °C
7: NaI / acetone / 2 h / Heating

References:

Riche, Francoise;Mathieu, Jean-Paul;Vincens, Maurice;Bardy, Andre;Comet, Michel;Vidal, Michel [Bulletin de la Societe Chimique de France,1984,vol. 2,# 1-2,p. 49 - 55]

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