ChemicalBook CAS DataBase List (2R,3S)-2-[(1R)-1-[3,5-Bis(trifluoroMethyl)phenyl]ethoxy]-3-(phenyl)Morpholine

(2R,3S)-2-[(1R)-1-[3,5-Bis(trifluoroMethyl)phenyl]ethoxy]-3-(phenyl)Morpholine synthesis

5synthesis methods

Product Name:(2R,3S)-2-[(1R)-1-[3,5-Bis(trifluoroMethyl)phenyl]ethoxy]-3-(phenyl)Morpholine
CAS Number:171338-33-3
Molecular formula:C20H19F6NO2
Molecular Weight:419.36

3,5-Bis(trifluoromethyl)benzoyl chloride

785-56-8
244 suppliers
$6.00/1g

(2R,3S)-2-[(1R)-1-[3,5-Bis(trifluoroMethyl)phenyl]ethoxy]-3-(phenyl)Morpholine

171338-33-3
12 suppliers
inquiry

Yield:-

Steps:

Multi-step reaction with 3 steps
1: 1.) L-Selectride / 1.) THF, -78 deg C, 45 min, 2.) THF, -78 deg C, 30 min
2: 69 percent / tetrahydrofuran; toluene / 18 h / Heating
3: 75 percent / H₂ / 10percent Pd/C / ethyl acetate; propan-2-ol / 48 h

References:

Hale, Jeffrey J.;Mills, Sander G.;MacCoss, Malcolm;Finke, Paul E.;Cascieri, Margaret A.;Sadowski, Sharon;Ber, Elzbieta;Chicchi, Gary G.;Kurtz, Marc;Metzger, Joseph;Eiermann, George;Tsou, Nancy N.;Tattersall, F. David;Rupniak, Nadia M. J.;Williams, Angela R.;Rycroft, Wayne;Hargreaves, Richard;MacIntyre, D. Euan [Journal of Medicinal Chemistry,1998,vol. 41,# 23,p. 4607 - 4614]

Morpholine, 2-[[1-[3,5-bis(trifluoromethyl)phenyl]ethenyl]oxy]-3-phenyl-4-(phenylmethyl)-, (2R,3S)-

170729-73-4
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170729-74-5
9 suppliers
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171338-33-3
12 suppliers
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References

100-58-3
196 suppliers
$18.00/10ml

(2R)-4-BENZYL-2-{(1R)-1-[3,5-BIS(TRIFLUOROMETHYL)PHENYL]ETHOXY}MORPHOLIN-3-ONE

287930-75-0
167 suppliers
$85.00/1g

171338-33-3
12 suppliers
inquiry

References

2-Morpholinone, 3-phenyl-4-(phenylmethyl)-, (3S)-

159706-35-1
0 suppliers
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171338-33-3
12 suppliers
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References

Benzoic acid, 3,5-bis(trifluoromethyl)-, (2R,3S)-3-phenyl-4-(phenylmethyl)-2-morpholinyl ester

170729-72-3
0 suppliers
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171338-33-3
12 suppliers
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References

(2R,3S)-2-[(1R)-1-[3,5-Bis(trifluoroMethyl)phenyl]ethoxy]-3-(phenyl)Morpholine Related Search:

Aprepitant Impurity 9 (R,R,R)-Aprepitant Aprepitant (2S,3R)-2-((S)-1-(3,5-bis(trifluoroMethyl)phenyl)ethoxy)-3-(4-fluorophenyl)Morpholine [2R-[2aR*),3a]-2-[1-[3,5-Bis(trifluoromethyl)phenyl]ethoxy]-3-(4-fluorophenyl)morpholine

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(2R,3S)-2-[(1R)-1-[3,5-Bis(trifluoroMethyl)phenyl]ethoxy]-3-(phenyl)Morpholine synthesis

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