(5beta)-3beta-[(2,6-dideoxy-beta-D-ribo-hexopyranosyl)oxy]-14-hydroxycard-20(22)-enolide synthesis
- Product Name:(5beta)-3beta-[(2,6-dideoxy-beta-D-ribo-hexopyranosyl)oxy]-14-hydroxycard-20(22)-enolide
- CAS Number:18404-43-8
- Molecular formula:C29H44O7
- Molecular Weight:504.66
![3beta-[[2,6-dideoxy-4-O-(2,6-dideoxy-beta-D\-ribo-hexopyranosyl)-beta-D\-ribo-hexopyranosyl]oxy]-14-hydroxy-5beta-card-20(22)-enolide](/CAS/GIF/16479-50-8.gif)
16479-50-8
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18404-43-8
8 suppliers
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Yield:18404-43-8 84%
Reaction Conditions:
Stage #1: digitoxigen O-[2',6'-dideoxy-β-D-ribo-hexopyranosyl]-(1->4)-(2,6-dideoxy-β-D-ribo-hexopyranoside)with sodium periodate in ethanol;water;
Stage #2: with methanol;sodium tetrahydroborate for 4 h;
Stage #3: with hydrogenchloride in methanol;water;
References:
Munkert, Jennifer;Santiago Franco, Marina;Nolte, Elke;Thaís Silva, Izabella;Oliveira Castilho, Rachel;Melo Ottoni, Flaviano;Schneider, Naira F. Z.;Oliveira, M?nica C.;Taubert, Helge;Bauer, Walter;Andrade, Saulo F.;Alves, Ricardo J.;Sim?es, Cláudia M. O.;Braga, Fern?o C.;Kreis, Wolfgang;De Pádua, Rodrigo Maia [Planta Medica,2017,vol. 83,# 12-13,p. 1035 - 1043]
71-63-6
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$43.00/100mg
18404-43-8
8 suppliers
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71-63-6
236 suppliers
$43.00/100mg
16479-50-8
3 suppliers
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18404-43-8
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143-62-4
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$43.00/5mg