Benzoic acid, 4-(trifluoromethyl)-, 1,1-dimethylethyl ester synthesis
- Product Name:Benzoic acid, 4-(trifluoromethyl)-, 1,1-dimethylethyl ester
- CAS Number:196934-20-0
- Molecular formula:C12H13F3O2
- Molecular Weight:246.23
455-14-1
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75-65-0
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196934-20-0
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Yield:196934-20-0 110.8 mg
Reaction Conditions:
Stage #1: 4-trifluoromethylphenylaminewith tetrafluoroboric acid;sodium nitrite in water at 0; for 0.75 h;
Stage #2: carbon monoxide;tert-butyl alcoholwith sodium formate in acetonitrile at 20; under 37503.8 Torr; for 3 h;
References:
Koziakov, Denis;Jacobi Von Wangelin, Axel [Organic and Biomolecular Chemistry,2017,vol. 15,# 32,p. 6715 - 6719] Location in patent:supporting information
201230-82-2
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402-43-7
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865-48-5
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$11.19/25G
196934-20-0
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455-19-6
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110-05-4
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196934-20-0
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540-88-5
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2967-66-0
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196934-20-0
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24424-99-5
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$13.50/25G
214360-65-3
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$9.00/1g
196934-20-0
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