2',2,2,5'-TETRAMETHYLPROPIOPHENONE synthesis
- Product Name:2',2,2,5'-TETRAMETHYLPROPIOPHENONE
- CAS Number:66390-56-5
- Molecular formula:C13H18O
- Molecular Weight:190.28
5445-46-5
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$527.00/1g
74-88-4
349 suppliers
$15.00/10g
66390-56-5
29 suppliers
$54.00/100mg
Yield:66390-56-5 77.9%
Reaction Conditions:
Stage #1: 1-(2,5-dimethylphenyl)-2-methyl-propane-1-onewith sodium hydride in tetrahydrofuran; for 1 h;Inert atmosphere;Reflux;
Stage #2: methyl iodide in tetrahydrofuran at 20 - 50;Inert atmosphere;
References:
Ding, Yi;Zhang, Yi;Li, Yongxin;Pullarkat, Sumod A.;Andrews, Paul;Leung, Pak-Hing [European Journal of Inorganic Chemistry,2010,# 28,p. 4427 - 4437] Location in patent:experimental part
106-42-3
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$20.00/25ML
3282-30-2
375 suppliers
$22.00/100ml
66390-56-5
29 suppliers
$54.00/100mg