2,2',4,4',5,5'-HEXACHLOROBIPHENYL synthesis
- Product Name:2,2',4,4',5,5'-HEXACHLOROBIPHENYL
- CAS Number:35065-27-1
- Molecular formula:C12H4Cl6
- Molecular Weight:360.88
108-86-1
516 suppliers
$10.00/5g
95-94-3
144 suppliers
$10.00/5g
92-52-4
419 suppliers
$9.00/5g
15862-07-4
48 suppliers
$55.00/1mg
35065-27-1
75 suppliers
$146.00/2ml
Yield:15862-07-4 52% ，92-52-4 16% ，35065-27-1 4%
Reaction Conditions:
Stage #1:bromobenzene with n-butyllithium in tetrahydrofuran;hexane for 0.333333 h;cooling;
Stage #2: with zinc(II) chloride in tetrahydrofuran;hexane at 20; for 0.333333 h;
Stage #3:1,2,4,5-tetrachlorobenzene;tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran;hexane for 24 h;Heating;Negishi coupling;
References:
Burukin;Vasil'ev;Chizhov;Zlotin [Russian Chemical Bulletin,2005,vol. 54,# 4,p. 970 - 974]
7145-82-6
67 suppliers
$9.00/5g
35065-27-1
75 suppliers
$146.00/2ml
35065-29-3
64 suppliers
$146.00/2ml
52712-04-6
28 suppliers
$155.00/1mg
35065-27-1
75 suppliers
$146.00/2ml
52663-72-6
36 suppliers
$502.89/5MG
636-30-6
227 suppliers
$31.00/25g
120-82-1
328 suppliers
$10.00/25g
35065-27-1
75 suppliers
$146.00/2ml
38380-04-0
38 suppliers
$134.00/5mg
35065-28-2
72 suppliers
$141.00/022-25mg
51908-16-8
27 suppliers
$240.00/0.5mg
636-30-6
227 suppliers
$31.00/25g
35065-27-1
75 suppliers
$146.00/2ml