2,2',4,4',6,6'-HEXABROMOBIPHENYL synthesis
- Product Name:2,2',4,4',6,6'-HEXABROMOBIPHENYL
- CAS Number:59261-08-4
- Molecular formula:C12H4Br6
- Molecular Weight:627.58
626-39-1
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59261-08-4
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Yield: 61%
Reaction Conditions:
Stage #1:1,3,5-trisbromobenzene with lithium diisopropyl amide in tetrahydrofuran;hexane at -78; for 2 h;Inert atmosphere;
Stage #2: with lithium chloride;copper(I) bromide in hexane at -78; for 2 h;Inert atmosphere;
Stage #3: with p-benzoquinone in tetrahydrofuran;hexane at -78 - 20; for 1 h;Inert atmosphere;
References:
Graff, Julien;Debande, Thibaut;Praz, Jezabel;Guenee, Laure;Alexakis, Alexandre [Organic Letters,2013,vol. 15,# 16,p. 4270 - 4273] Location in patent:supporting information
21521-51-7
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59261-08-4
35 suppliers
$185.00/25mg