2,2-Dimethylbutane synthesis
- Product Name:2,2-Dimethylbutane
- CAS Number:75-83-2
- Molecular formula:C6H14
- Molecular Weight:86.18
110-54-3
826 suppliers
$20.00/100ml
96-14-0
105 suppliers
$22.19/5ml
107-83-5
242 suppliers
$10.00/1g
75-83-2
128 suppliers
$35.00/1ml
79-29-8
138 suppliers
$20.00/1g
Yield:79-29-8 8% ，75-83-2 6.7%
Reaction Conditions:
with hydrogen at 215; under 7500.75 Torr;Catalytic behavior;Kinetics;Flow reactor;Overall yield = 62.1 %;Reagent/catalyst;Temperature;
Steps:
2.3. Kinetic analysis
The conversions and yields of branched hexane isomers andlower molecular weight by-products were also analyzed underprocess-like conditions. These catalytic tests were performed usinga stainless-steel gas flow tubular PID Eng&Tech Microactivity - Ref-erence reactor at a pressure of 10 bar with a H2to hexane molarratio of 6 and amount of catalyst equal to 2.5 g (5 ml) with a flowrate corresponding to WHSV 0.7 h-1and GHSV 638 h-1. The tem-perature was controlled by an internal thermocouple and kept atthe desired temperature in the range 200-215C. Liquid n-hexanewas continuously loaded by a Gilson 307 pressure pump and evap-orated in the hot flow of hydrogen gas. The reaction productswere analyzed using an on-line connected Perkin Elmer Clarus580 gas chromatograph equipped with CP-Sil Pona CB column(100 m × 0.25 mm × 0.5 m) and a FID detector.
References:
Sazama, Petr;Kaucky, Dalibor;Moravkova, Jaroslava;Pilar, Radim;Klein, Petr;Pastvova, Jana;Tabor, Edyta;Sklenak, Stepan;Jakubec, Ivo;Mokrzycki, Lukasz [Applied Catalysis A: General,2017,vol. 533,p. 28 - 37]
558-37-2
164 suppliers
$10.00/5g
75-83-2
128 suppliers
$35.00/1ml
75-97-8
238 suppliers
$10.00/1g
75-83-2
128 suppliers
$35.00/1ml
558-37-2
164 suppliers
$10.00/5g
201230-82-2
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75-83-2
128 suppliers
$35.00/1ml
926-36-3
7 suppliers
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110-54-3
826 suppliers
$20.00/100ml
75-83-2
128 suppliers
$35.00/1ml
79-29-8
138 suppliers
$20.00/1g