2-(2-NITRO-PHENOXY)-PROPIONIC ACID ETHYL ESTER synthesis
3synthesis methods
- Product Name:2-(2-NITRO-PHENOXY)-PROPIONIC ACID ETHYL ESTER
- CAS Number:13212-56-1
- Molecular formula:C11H13NO5
- Molecular Weight:239.22
Yield:13212-56-1 99%
Reaction Conditions:
Stage #1: 2-hydroxynitrobenzenewith potassium hydroxide in ethanol; for 0.5 h;
Stage #2: Ethyl 2-bromopropionate in N,N-dimethyl-formamide; for 16 h;Inert atmosphere;
References:
Macias, Francisco A.;Chinchilla, Nuria;Varela, Rosa M.;Molinillo, Jose M. G.;Marin, David;De Siqueira, Joao M. [Journal of Agricultural and Food Chemistry,2008,vol. 56,# 21,p. 9941 - 9948] Location in patent:experimental part
