2,4-DIMETHYLPHENYL ISOCYANATE synthesis
- Product Name:2,4-DIMETHYLPHENYL ISOCYANATE
- CAS Number:51163-29-2
- Molecular formula:C9H9NO
- Molecular Weight:147.17
32315-10-9
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95-68-1
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51163-29-2
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Yield:-
Reaction Conditions:
in 1,4-dioxane;Reflux;
Steps:
3.4. General Procedure for Preparation of Aromatic Isocyanates (6a-n)
General procedure: Appropriate aromatic amine (0.02 mol) was added slowly to a stirred solution of BTC (3.0 g,0.01 mol) in 1,4-dioxane (30 mL) at room temperature. After refluxing for 8-12 h, excess 1,4-dioxanewas evaporated. The residue was distilled under reduced pressure to afford compounds 6a-n.
References:
Jiang, Nan;Bu, Yanxin;Wang, Yu;Nie, Minhua;Zhang, Dajun;Zhai, Xin [Molecules,2016,vol. 21,# 11,art. no. 1572]
2990-02-5
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51163-29-2
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35601-95-7
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51163-29-2
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