2,5-Dihydroxyterephthalic acid synthesis
- Product Name:2,5-Dihydroxyterephthalic acid
- CAS Number:610-92-4
- Molecular formula:C8H6O6
- Molecular Weight:198.13
106-42-3
435 suppliers
$18.00/25ML
610-92-4
284 suppliers
$6.00/1g
Yield:610-92-4 80.6%
Reaction Conditions:
with dihydrogen peroxide;trifluoroacetic acid in ethanol at 90; for 10 h;Temperature;Reagent/catalyst;Solvent;
Steps:
1-10 Example IV:
Pipette 2.5mL (≈20mmol) of p-xylene into a 100mL round-bottomed flask, and add Cu-MCM41 (0.20g, Cu content of 10percent), ethanol (17mL), trifluoroacetic acid (3mL), hydrogen peroxide (30percent) in sequence , 7mL), after reacting at 90°C for 10h, stop the reaction, cool, filter, and separate to obtain 3.0g (separated yield is about 80.6percent) of 2,5-dihydroxyterephthalic acid.
References:
Yunnan University;Wang Jiaqiang;Li Ying;Yan Zhiying;Wu Mingzhu;Li Zhiqiang;Jiang Liang CN104829449, 2020, B Location in patent:Paragraph 0006-0026
13731-82-3
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$7.00/1g
636-94-2
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$7.00/100mg
610-92-4
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$6.00/1g
13731-82-3
206 suppliers
$7.00/1g
610-92-4
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$6.00/1g
13799-90-1
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$5.00/250mg
610-92-4
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$6.00/1g
5870-38-2
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$25.00/1g
610-92-4
284 suppliers
$6.00/1g